open access publication

Article, 2024

Recovery of dislocation cell structures in 316L stainless steel manufactured by selective laser melting

Journal of Materials Research and Technology, ISSN 2214-0697, 2238-7854, Volume 30, Pages 9472-9480, 10.1016/j.jmrt.2024.05.269

Contributors

Fan, Jinming [1] Zhu, Yueyue [1] Wang, Weiyi [2] Chen, Ke [1] Godfrey, Andrew-William 0000-0002-5496-0424 [2] Yu, Tian Bo 0000-0001-9525-9354 (Corresponding author) [3] Huang, Xiaoxu (Corresponding author) [1]

Affiliations

  1. [1] Chongqing University
  2. [NORA names: China; Asia, East];
  3. [2] Tsinghua University
  4. [NORA names: China; Asia, East];
  5. [3] Technical University of Denmark
  6. [NORA names: DTU Technical University of Denmark; University; Denmark; Europe, EU; Nordic; OECD]

Abstract

Understanding the recovery mechanism associated with the dislocation cell structure in 316L austenitic stainless steel produced by selective laser melting (SLM), as well as the role played by the accompanying segregation network, is crucial for tailoring the microstructures and mechanical properties of SLM-prepared components. In the present work, the evolution of the dislocation cells was investigated during isothermal annealing, and a recovery mechanism for the dislocation cell structure was proposed based on a combination of microstructural observations and recovery kinetics analysis. The results show that the high-density dislocations at the cell boundaries annihilate during prolonged annealing at 800 °C, resulting in the decomposition of the dislocation cells. The recovery kinetics analysis reveals that SLM-prepared 316L exhibits a lower recovery rate and requires significantly higher apparent activation energy during annealing compared to conventional 316L deformed by cold rolling. The segregation network plays an important role during the dislocation recovery process, which limits the dislocation reaction occurring within the cell boundaries at the early stage of recovery, impedes the dislocation motion after the decomposition of dislocation cells, and leads to a strong temperature dependence of recovery kinetics in SLM-prepared 316L.

Keywords

SLM, activation energy, analysis, annealing, apparent activation energy, austenitic stainless steel, boundaries, cell boundaries, cell structure, cells, cold rolling, combination, combination of microstructural observations, components, conventional 316L, decomposition, dislocation, dislocation cell structure, dislocation cells, dislocation motion, dislocation reactions, dislocation recovery processes, early stages, early stages of recovery, energy, evolution, high-density dislocations, isothermal annealing, kinetic analysis, kinetics, laser, laser melting, mechanical properties, mechanism, melting, microstructural observations, microstructure, motion, network, observations, process, prolonged annealing, rate, reaction, recovery, recovery kinetics, recovery mechanism, recovery process, recovery rate, results, rolling, segregated network, segregation, stages of recovery, stainless steel, steel, strong temperature dependence, structure

Funders

  • National Natural Science Foundation of China

Data Provider: Digital Science