Article, 2024

Assessment of Residual Stress Behavior and Material Properties in Steels Produced via Oxynitrocarburized Metal Injection Molding

Journal of Materials Engineering and Performance, ISSN 1544-1024, 1059-9495, Pages 1-6, 10.1007/s11665-024-09401-x

Contributors

Medeiros, Jorge Luis Braz [1] Biehl, Luciano Volcanoglo [1] Martins, Carlos Otávio Damas [2] de Jesus Pacheco, Diego Augusto (Corresponding author) [3] de Souza, José [1] Reguly, Afonso [1]

Affiliations

  1. [1] Federal University of Rio Grande do Sul
  2. [NORA names: Brazil; America, South];
  3. [2] Universidade Federal de Sergipe
  4. [NORA names: Brazil; America, South];
  5. [3] Aarhus University
  6. [NORA names: AU Aarhus University; University; Denmark; Europe, EU; Nordic; OECD]

Abstract

By combining the formability of injection-molded polymers with a wide range of metal options, metal injection molding (MIM) allows for manufacturing metallic components with small dimensions and complex geometries. However, steels produced through this process often exhibit higher porosity compared to conventional methods. This article aims to fill this gap by developing a thermochemical oxynitrocarburizing treatment cycle applied to the austenitic stainless steel Catamold 316L. The developed treatment analyzes the diffusion kinetics, mechanical properties, and metallurgical behavior. The oxynitrocarburizing treatment was carried out at a temperature of 570 °C for varying durations of 30, 60, and 120 min. The findings showed that surface microhardness significantly increased, and corrosion resistance improved due to the ceramic behavior of the Epsolon composite and the formation of magnetite, compared to the sintered material. The study reveals a substantial rise in residual compressive stresses of up to − 2790 MPa on the sample surface. The residual stress values and the elevated surface microhardness are highly beneficial for improving the tribological properties of Catamold 316L steel produced by the MIM process. The study suggests that using ionic oxynitrocarburizing in salt baths presents an alternative to plasma processes for treating Catamold 316L steel, providing improved diffusion of nitrogen and carbon.

Keywords

MPa, alternative, article, assessment, bath, behavior, carbon, ceramic behavior, complex geometries, components, compressive stress, conventional methods, corrosion, corrosion resistance, cycle, diffusion, diffusion kinetics, diffusion of nitrogen, dimensions, duration, findings, formability, formation, formation of magnetite, geometry, improved diffusion, injection molding, injection-molded polymer, kinetics, magnetite, manufactured metallic components, material properties, materials, mechanical properties, metal, metal components, metal injection molding, metal injection molding process, metal option, metallurgical behavior, method, microhardness, mold, nitrogen, options, plasma process, polymer, porosity, process, properties, residual compressive stress, residual stress behavior, residual stress values, resistance, salt, salt bath, sample surface, samples, sintered materials, steel, stress, stress behavior, stress values, study, surface, surface microhardness, temperature, treatment, treatment cycles, tribological properties, values

Data Provider: Digital Science