open access publication

Article, 2024

Analysis of slip transfer across grain boundaries in Ti via diffraction contrast tomography and high-resolution digital image correlation: When the geometrical criteria are not sufficient

International Journal of Plasticity, ISSN 0749-6419, 1879-2154, Volume 175, Page 103941, 10.1016/j.ijplas.2024.103941

Contributors

Nieto-Valeiras, Eugenia 0000-0003-4957-1675 [1] [2] Orozco-Caballero, Alberto 0000-0001-9518-8816 [1] [2] Sarebanzadeh, Maral [1] [2] Sun, J. [3] Llorca, Javier 0000-0002-3122-7879 (Corresponding author) [1] [2]

Affiliations

  1. [1] IMDEA Materials
  2. [NORA names: Spain; Europe, EU; OECD];
  3. [2] Technical University of Madrid
  4. [NORA names: Spain; Europe, EU; OECD];
  5. [3] Xnovo Technology ApS, DK-4600 Køge, Denmark
  6. [NORA names: Denmark; Europe, EU; Nordic; OECD]

Abstract

High-resolution digital image correlation was employed to analyze the occurrence of slip transfer across grain boundaries in pure Ti. The microstructure was characterized in 3D through diffraction contrast tomography and electron backscatter diffraction. The prismatic slip activity was captured in the shear strain maps at different strains, and the grain boundaries were classified according to the occurrence/absence of slip transfer. Different geometrical slip transfer criteria were tested, and, in general, the slip transfer likelihood increased when the slip systems across the boundary were well-aligned. Nevertheless, a detailed analysis of selected grain boundaries revealed that slip transfer could be triggered or impeded depending on the local stresses acting on the neighborhood, regardless of the alignment between the slip systems. The microstructural and deformation patterns where the geometrical criteria are not enough to predict slip transfer are assessed.

Keywords

Ti, activity, alignment, analysis, backscatter diffraction, boundaries, contrast tomography, correlation, criteria, deformation, deformation patterns, diffraction, diffraction contrast tomography, digital image correlation, electron, electron backscatter diffraction, geometric criteria, grain, grain boundaries, high-resolution digital image correlation, image correlation, likelihood, local stress, maps, microstructure, neighborhood, occurrence, occurrence/absence, patterns, prismatic slip activity, shear, shear strain maps, slip, slip activity, slip systems, slip transfer, strain, strain maps, stress, system, tomography, transfer, transfer criteria

Funders

  • European Commission
  • Comunidad de Madrid

Data Provider: Digital Science