open access publication

Article, 2022

Thermochemical post-processing of additively manufactured austenitic stainless steel

Surface and Coatings Technology, ISSN 1879-3347, 0257-8972, Volume 441, Page 128495, 10.1016/j.surfcoat.2022.128495

Contributors

Funch, Cecilie Vase 0000-0002-3114-5793 (Corresponding author) [1] Somlo, Kinga 0000-0002-3459-0657 [1] Christiansen, Thomas Lundin 0000-0001-7144-1557 [1] Somers, Marcel Adrianius Johannes 0000-0001-7773-1432 [1]

Affiliations

  1. [1] Technical University of Denmark
  2. [NORA names: DTU Technical University of Denmark; University; Denmark; Europe, EU; Nordic; OECD]

Abstract

The effects of different thermochemical post-processing treatments on the microstructure and properties of additively manufactured austenitic stainless steel were investigated. If the nitrogen content in the as-built condition is high, austenitization in vacuum causes a reduction in nitrogen content near the surface. This can be remedied by applying a small amount of nitrogen in the gas during austenitization. Using high temperature solution nitriding, the surface hardness could be effectively raised by deliberate nitrogen ingress, while maintaining a very fine structure inside the primary austenite grains. The excellent combination of strength and ductility of the as-built condition is accompanied by a low degree of work-hardening. This condition showed elastic and plastic anisotropy. The vertically built condition exhibits a lower strength and an early initiation of yielding as compared to the horizontally built conditions. High temperature treatments were able to efficiently reduce the mechanical anisotropy exhibited in the as-built condition. A combination of high- and low temperature surface hardening was investigated using nitriding, carburizing and nitrocarburizing. In all cases expanded austenite developed on the surface, which created a strong hardness increase.

Keywords

amount, amount of nitrogen, anisotropy, as-built condition, austenite, austenite grains, austenitic stainless steel, carburization, cases, combination, combination of strength, conditions, content, degree of work-hardening, ductility, early initiation, effect, excellent combination, excellent combination of strength, gas, grain, hardening, hardness, hardness increase, high-temperature treatment, increase, ingress, initiation, low degree, low temperature surface hardening, manufactured austenitic stainless steel, mechanical anisotropy, microstructure, nitride, nitrocarburizing, nitrogen, nitrogen content, plastic anisotropy, post-processing, post-processing treatments, primary austenite grains, properties, reduction, solution nitriding, stainless steel, steel, strength, surface, surface hardening, surface hardness, temperature, temperature treatment, treatment, vacuum, work hardening

Funders

  • Innovation Fund Denmark

Data Provider: Digital Science